position | δH (mult, J in HZ) | δC (DEPT) | H–H COSY | HMBC |
---|---|---|---|---|
1 | Â | 202.82 | Â | Â |
2 | 6.08 (1H, d, J = 9.87) | 131.97 (CH) | H-3, H-4 | C-1, C-3, C-4, C-10 |
3 | 6.96 (1H, dd, J = 9.2, 6.2) | 143.66 (CH) | H-2, H-4 | C-1, C-4, C-5 |
4 | 3.56 (1H, d, J = 6.10) | 69.71 (CH) | H-2, H3 | C-2, C-3, C-10 |
5 | Â | 63.41 | Â | Â |
6 | 3.11 (1H, brs) | 60.57 (CH) | Â | C-4, C-7, C-8 |
7 | Â | 29.09 (CH2) | Â | Â |
8 | Â | 33.8 (CH) | Â | Â |
9 | Â | 37.06 (CH) | Â | Â |
10 | Â | 49.0 | Â | Â |
11 | Â | 25.81 (CH2) | Â | Â |
12 | Â | 29.62 (CH2) | Â | Â |
13 | Â | 54.11 | Â | Â |
14 | Â | 82.46 | Â | Â |
15 | Â | 31.80 (CH2) | Â | Â |
16 | Â | 36.78 (CH2) | Â | Â |
17 | Â | 87.22 | Â | Â |
18 | 1.18 (3H, S) | 19.21 (CH3) | Â | Â |
19 | 1.26 (3H, S) | 15.23 (CH3) | Â | Â |
20 | Â | 78.42 | Â | Â |
21 | 1.29 (3H, S) | 18.03 (CH3) | Â | Â |
22 | 4.80 (1H, m) | 81.43 (CH) | Â | Â |
23 | Â | 34.25 (CH2) | Â | Â |
24 | Â | 152.10 | Â | Â |
25 | Â | 120.51 | Â | Â |
26 | Â | 167.68 | Â | Â |
27 | 1.86 (3H, S) | 13.02 (CH3) | Â | Â |
28 | 1.74 (3H, S) | 10.98 (CH3) | Â | Â |